1、 r A M E _ Q V _ s d 2. + v “ , + null 610064)null null K null 1 : r A M (HPLC) V _ s d s ;V _ s d , V ns ; _ : SPD- 1; ) : C-R6A ; V CTO- 2AS bnull null : ZORBAX. SIL A ; 4. 6 mm ! 25cm;null null _ o : 254 nmb1. 2null k 4null null s d 2. 3.4. CHP;5. j ? ;6. ( / )m 1null = B c = H W Ynull null V m V
2、 A , J ? 1 9 F , = H W b J ? M 1 2 % H F z =H W 1 z b M - a= B J ? 1 (V/V 90null8null2) R b109 null null null null null null null null null 2000 M 2 a 2 s p “ null null null null null null null null null null null nullm 2null J ? c = H W Y2. 2null V 4null null L , , = H W h l , s , 35 H n y 0 s v b7
3、 O - m , V 3 , L , Z E2 / by N , 8 I n 35 , e M 1 mL/minb2. 3null S w Lnull null G H q k T , 4 H q : M X := B nullJ ? = 90null8null2; 35 , e M 1 mL/minbnull null F s i S A , A : U S , i U S T m bV m 3 V A , S w L 0. 2 2. 2 g/L S L bm 3null S w L2. 4null Z E null null H q / , i CHP A i “ 5Q , Q 10 mL
4、, 9 i ( Z E b T A U , CHP i 0. 25 2. 0 g/ LS = , M s “ z 1 %b2. 5null Q 8 “ s null null m 4 Q 8 “ HPLC m , V m V A 4 H q , V P CHPQ 8 “ z s bm 4null Q 8 “ m HPLC s E s Y Q 8 “ CHP, H | “ , CHP i 0. 25 2.0g/ LS ,s T V ,Z E W ( 0.7 %,= z b HPLC1 s E e Ly bnull null : r A M E V _ s d& CHPQ 8 “ Q s ,ZOR
5、BAX. SILA , - null= B nullJ ?= 90null8null2 A M , 35 , e M 1 mL/min,Q 8 “ F s ? H a y s , CHP i 0. 25 2. 0 g/LS = ,M s “ z 1 %bN E y e L , ? L L H S e , s r b I D :1 null Bosoh Elisabeth et al, Anal. Chim. Acta, 1994, 299( 2):219.2 null Hennion Marie- Claire et al, J. Chromatogr. , A, 1995,712(2): 2
6、87.3 null null , null r . r A M E 1 . : 2 S / ,1980.4 null s m ( s ). : ,1984.Determination of Synthetic Reaction Product PropylbenzeneHydroperoxide by HPLCXIANG Ruinullli, ZH U Xiaonullhong, K UANG Denullzhong(T esting and Analytical Centre,Sichuan University,Chengdu 610064, China)110null null null null null null null null null null null null 2000 M 2 a 2 s p “ null null null null null null null null null
