1、ICS 73.040D 21GB/T 476-2008Tt GB/T 476-2001, GB/T 15460-2003, GB/T 18856. 11-2002i 1 -rLIJc p JiJlj E. J7 ip7K(ISO 625:1996, Solid mineral fuels-Determination of carbon andhydrogen-Liebig method, MOD)2008-07-29 - 2009-05-01 r*-IVGB/T 476-2008r7 3 (ik % A=i k ) 1 FtAf ISO 625 : 1996 ( E)(1* VA 4 -fN
2、j( ,1irl)(199GCX ), T 4 +() ISO 625:1996 7x#iL1giA)i l rfk 10M TTPlqE ,igip!J rp%M Wrrl-:1tf l1N*f;TA1*MTM-Ai%e t 1 tL3R , A f4 Rff A r9 tt T*#%r -r7 ISO 625:1996 4.0, 5(,fR-s J C l7 h, ISO 625 : 1996 Hf t%TI f T- I-Lb 1 Co ItAAP-toA113C,rp*74 V GB/T 476 -2001 ( ) W J , - c tT)%h),PM 3 * -A GB/T 154
3、60-2003(4fP%Oij 5tAW, *, I ) *n GB/ T 18856.11-2002(vKl f i - I1 X53 :7K1I i ijifAf )orl kj GB/T 476-2001 1 Ark, xT (A Ft1.1 ho 7J 5 ( i71,X J T m T* #%r a , Mfin , J # #%TfJ hG t iC h X33 3LGB/T 2121998, NEQ)J I J r * (GB/T 212-2008, ISO 11722:1999, 1 1171: 1997 ,ISO 562:GB/T 218 Jci (TcjiJ11 %(GB/
4、T 218-19ga:GB/T18856.1 7kiA-Aji71 X1 aSr:*3 -=i PMfQ-i 5ISO 925:1980)3. 1 1Tfig-h1-c7kJ# Gtr)tc77knT-59Ac7kiJAufz fn l Lk-S Q(.,r - V)pvp MA5 it R- iJi f o XXf Ok, iffl -4t4t4i f o3.2 it -PJn 43.2.1 7k :r1 #frf , lx 1 mm-3 mnm; :X*X t : jj Tj tl, VV 2 mm-5 mm,3.2.2 VN) X kl:ftf*t,-M fflAt t AilOff$l
5、-l 1 1J#o )nJJAA 10 mL(1+1)1 Leo ffCTJA 70 C80 Cf#t 5 min,T JH1k,JuW. 2 h-3 h, 7k;(1kJaI din 1a,f7kT,InliSC=f +, 150 C:T d“g“ 2 h-3 0. 5 rim-2 mm 4Mo3.2.3 Cyk-S:LkAjl 0. 5 mm, ykn:O. 15 mm(100 H),3.2.4 A*t,tA4K(-r-,M 5 mm),3.2.5 f“:r#frJhI 1 mm-4 mm,1i :fir J “e“nd i 7kilpJfiG ITC,#irrhjG i ftA_0P+,
6、1t 850 C-FMVE 2 h,IJX,L8z3.2.60. 25 mm,3.2.7VLL :99.9Yo ,aliJ3Rc p7illT - lniM k9V A ltf7fiIt)JKt (J1sfF1TJl)a3.2.8 EA,QMA:3Jfr9o3.2.9 1 mm-2 mm; J1u j ff : T Ix 0. 5 mm-2 mni,1GB/T 476-20083.2. 10 A .rrf Ho3.2.11 nIJ:TfRi kpA,1nfioli%iA F:4 100 gk*-qn 4-1pf1.yz y ;7-CTh1j7;, g9 -WAS;10 f7)UffM11 .a
7、z XTktUjf ;12-0k gkq -XI-L U jf ;13- .UJfs;14 it15 qJX1Ye11 -P p K I !IIJ z 5 min, t; iMy( A1I1 53.4. 3.2 8l,1 5 plrT.4GB/T 476-20082j _ U )k7 )K3 4 51 r r 6170 100 310 10 120 10 801-Ix ;2ykt ;3,5- J I7 f1 ;15 - i?1T Illr-k 3.4.3. 1 kn - Jt9 10 mm #A- 9 100 mm ffjC L-S,4 j 100 H fujLkIg9hJG-7 of 12j
8、i )1 34( GJ5ff.1 fA JA A.3.4.4 i t pJ TX 1IrtT- Cr,J AE! M( -lYX) j N-3ARM , fs A, Xp ,Iz IjAYmmi1-JtItft UP Mft , fg- MA 1 h. A ). (r 1 fpJ ff, If q fm i rh # , =1 #lkiJpli7YIJ#;t immft #hffIlml 5 min. iETM-_ft li pV),1 Js $J Ymmo3.4.5i11XrrJITx 1 1r # I , h U J Q ,14x 1 , # z ; iA ALL AL _lp_120 m
9、L / mino lA l J a t%i U Q RIIX C (iLl4 20 mL /min UT ,tk H)l /-tr ,eA MtHff7T A f-k,N U OA Q rP1PP 1?(60010) C ,4ft - I PV, M -V P o3.5. 1.2 r IN ckI d0 M;Mq d,IRVL /1, T 0. 2 mm 0I- f1 1Tr 1 “J“A Tait# 0. 2 g,0.000 2 g,3 j=1 it - 1 = AI-EQ. 7W it1tWJX kA 3- rT A jflWjM Q/kll=i1 GB/T 18856. 1 $113.5
10、. 1.3 IkIBfff, fl-,VV , 094k*-1, U 120 mL/min M, J)iLRAA IT 3f IJx ,JR$A4k-?tI)J 120 mL/min, 1 min)Ar-V7 k -4ity-vXP, A -fl A -;- p1A itJ ,1 1 k lbP 2 min )A ,T I k 1J1rP a gfflm 18 minF -p QJ-20L. 2 minia,IV -FO A pit7K1VrPfA tiJT1#c(4)1J(5)it:C 100-MCWM .(4 )cwM = Cold 100-M:,afl*51f) (-7K) T it )
11、rpVxAl 2 CC, o;-f74tT 1 J ( lKk i4ff) l:P RAI 3)t,o;-i 511T 1 1 , fi (g)-1xC-(T UJ1 ,1J5 (g);-I7K u0th,*,ft)iA(g);- Vr)7K T?( GB/T 212Il i )t11;2 (,-r7K1Fr hC Vi il1a lJl ej, r (3) tX-9 jW(C,_,l)WJ 3t:C-d = 0.272 97n, X 100-0.272 9(C02)a .(3 )6GB/T 476-2008HcwM - H,a X 100 - MCWM100-MACCWMCad -HCWM-
12、H,a-MCWM-MAa -7k1l; FR n4/J 100 mmA#OA%FT= M 8 mm, M lgh 6 mm,Kg$ 50 mm 0, i - lF (=J 7 mm, M llM 3 mm,KgJ40 mmWU 4Tl;ff f (,QM 7)650NN40tii1007 ?J 9 %r 914. 3.2.3 70 mm-77 mm )1-o fffitffl a M, 850 CTn, A 2 h,4.3.2.4#fiJ1xUul 8)a) # : Tz4J 2 mm, f 700 mm,-t ehjGATjM, 10 mmb) RR o $c) ft V, fkJ(z41
13、6 mm,F41M, 11 mmod) :jFgy4j 7 mm, kA 60 mmoe):4 o - t 1X 6mm ,7JL 7 mm;.7rkrk* ri , 2 I1*;3-WJ 41I4.3.4 ,Ut f;:FP- fr+ L 50 mA 700 mA fyJ 0. 001 mg4.3.5 Al Jet -:rp7 3.3. 1. 3,4.3.6 n 3.3.204.4 ut-4. 4. 1 * ft * f#c * ?a M, 3t AINIIf4. 4. 1. 1 rOTJ; M fkl i fA 9JC J2809 Pt-PZO53280 mm,llZxJoor4. 4.
14、1. 2 3 %EEC J*TA I 1_7 l“)1 fp7( Ix -t JA c f-5 lS-,wa sfQi *-“-4. 4. 1. 3 M 6 )frT)I4. 4.2 0, 3!E AAM, n M, it 3t !-J 10 mm t , r1 AM, 100 mm A f t,A 4-4 tIA10 mm ,JIA 10fi1r7:, * 5 1 T x FAQ k hK k i,1“P1v. t %K100 10I 10 ?k T I9GB/T 476-20084.5.1 9 fr*_NP,f) AT- ATL_# 1 711 A 3#%I4%i1i.jiJaJ Pjj7
15、 80 mL/min,# : . 1/JC,4.5.2 3t mipJuf,# Aht C Tk U (T!t 14u Bff q ff)8)fu:c ti-f-IfN x%L 19#4M80 mI,/min, F 7 (G JI ) ? o P )A ,r4FA 2 min-3 min -ZX *_ ( $J ) o10 min IA 1Y JC Tk c U : , c11J U 3f: 1 1 ifC 10 mine , rl o )a44 -rJ tAfH J ,VY_I Wra, M I-ALCATt FUffiV #1 crft-T, A 311 0.000 5 g f.4.5.3
16、 rklikkt,Y*(J;Xfp(1ktYIJ1#ia1or1lJ;%J,J t LJ JJ-J= 0.2 mm 11J-f) , ) 0.070 g-0.075 g, J%J 0. 000 2 g,M.-_1 -_ t o PuT_ 0P )J A-f , F, # klk 3 1T 1 1J J IJI i f o4. 5. 4 lTc U 80 mL/min, )4i 1 ,! l o1p531r1af1711cio #TF#JJJJ,k3rC.kqJ fc M4 #I r,AA,1 A, - A XtV8 q o 0 98 JQ (-fJC 30 s) , 1 ( GJJn ) l
17、k F f2i, $ 3 A q, 2 mine, l k 3 FFU V4A_ PRM4.5.5 gJ10minJA( IJ4c TJQIJ Ecu l7), XTplxt (TcU:f, ITAQ10 mi n Ja ,rho 2 I A q _ Tt U ff f J _, 1-L /J,T o. 000 5 g, it H4.4.3 - TARO 11#J%hTz1 5 mm 0, V VgfHbt75 PJi U W_N Itk v ri 1,ju Ff NAN fG /JAY1JF,ti ,AFt itL 9 4 1 -S 1 , J 3J% c co- r_t 4z a VA 9
18、1 a4.4.45aJAz41n 4.3. 5 0 4Y, A 6 llJQ TT- j4: ft q , X Z 7O ft r fJ 0, 1171-:1 C Z ua)xjiu,sK2-1nJXC1tU:IIJta VIX mgl1.HJ,Iu!_l#11 UJf:;b) f f-Ljt 7J K, J gj fu 7k It - i 1 M 9 ,L rA . IR /k U FP 0 X ft 3fM A V It # IiJI V“I =C f* A u41i X 4 ; .c) 1j, 7 L1pM 100 IX ItE ti n 4 I , _10aq JrT M) I III
19、T1 M4.4.51A i X C Ail IM 80 mL/min, It J 3. 4. 53.4.6 #Tj-,1E1 rJ,4Y 0. 070 g-0. 075 g d,il# c , rJ 7 0. 000 2 g,4.5 uxt_rI%54. 4. 6 ra 9I PToItJka10tiLcir.TklJfJ) I(mg) #7“#1kIJJX , yJXi3,IGB/T 476-20080 41 obv- , C f ; 1 #JJ # kn #J1 yJ A A;R . NP #kQ JJ f$9 min )a J 1 yc iE *,2 ,l , , , %) -1 (mg
20、)o IAJizA A-i M 415 M. n Mz fft f HAT- Mil 0.050 mg,KX MiIi.M 5if (h*t=1Jft i 90 E Mo4.5.7 7TTfit#J;JLJJ0 N9(xOT (i3A5#Lhi 7Jmfo4.6 a iit4.6.1 1 * n tX- 3V7)( 7j,Ai TAi4 )0 (Caa )fn ,(Haa )%I3 C -(1) :H.a = M2 - s X 100-0. 111 9M d . ( 6 )it, X 1 000A+:n72 q2V 1,TJ( , T1 J (mg);nn2 Q TJ , Tl J A(mg)
21、o !J #I1 6 , rt(3)it 11 cJIAI.ftOC,4.6.2n 3. 6. 2,5 *i i-AwfA it J 1 I 1 I Im r 1 An o1 IAi1It M1IftW I/ Yo 111h Wk-Ca H., Ca H,0. 50 0. 15 1.00 0. 256 VA n, 4911GB/T 476-2008Rf A A( YI *4IIRtA)5 ISO 625:1996 “IFA. 1 yaLh -j ISO 625:1996 *A XI -%A,A A. 1 * r% s -5 ISO 625:1996 i,A-9yX4977r ISO 625:
22、19967ti31 12 23.1 33. 2 43.2.1 4.1423.2.2 4. 33. 4.63. 2. 1353. 3. 1. 2a) 5. 3. 13. 3. 1. 2b) 5. 3. 23.3.1.3 5.43.3. 1. 3b) 5.4(d)3.4 673.4.7 63. 5. 1 g3. 6 104 -5 116 1212GB/T 476-2008A B( ItNtA)ISO 625:1996 #Irxl*7B. 1 T S ISO 625:1996 1 #1 1 _P-B. 1ISO 625: 1996 #IT1$C#r 3,s 7 qA* L A14 Y N1% 1bM
23、 a1P AAMhnTv mi /X 1F, W-1 . i t01 iiRILIA IRrfrJfi /1L1 1L 1 i- :1 it2 5ImTAm VT1VT1711 7 N 7LP 116 16 4I 1ti a P), .01 R. Pd FAIN3.2.1 71Cir ( f JQ r j1: * Tk “i; 11f151; i4 -Q?. I iA 3i 11 J 7 a- )i111 1t1 ISO 625:1996 illIYJi. 11111,H:1:4 4.2 yfdJLiJi 11 4,/ fJN4011/11*i:1116AUU 13.2.2 1 6 ISO 6
24、25 : 1996 A,(1;ffiM$11 Jill 51iialXkl -f q 7#m(FIt3.2.5 +Tafah ITxI% Zi“iJ t 911 JA-3,3. 2. 8 - 3 . 2. 13 r71f1 j11M, i 4 J A I fnifL i o$Z ISO 625: 1996 L1 5. 3. 1 M, 1 I1 Sf13.3. 1.2a ) 20 mm-150 mm,- 14 7 75 1x ( J 850 Jtj 0 LA 111-1 1919f1IJI r =i 14 ISO 625: 1996 F 1 5. 3. 2) J 1z X1173.3.1.2b
25、) :iiR N fIIq20 nim- 22 mmISO 6 2 5 : 1996 1 I T 5 . 4 1K qk frr. g j t 1)1 I J 11 4Y i f IJII51l it P . 1141 fl 1:3.3.1.344 ISO 625:1996 uP 5.4 d )ahcqX = E iA 11 t3.3. 1. 3b) 11A5 i rjW H%I ISO 625:1996 r 8 0 *J9:1 . ,L 1itI1JAt, Y3.5.1 120 mL/min;2. tl i49- j - 11%ItY11. 3. W Pa iiT 1111190 (rj A
26、7# 1 NkHtl914 ISO sc 111;)j1k,*vTT71 1x1111 1 1 -_ 11, A- M- ( Mek ISO 625: 1996 l 11“ )x“ ( X1 L 1n15 J, it, n It 14 0 Fri13http:/GB/T 476-20081 q *; : -6 1x1-,I, p7i7 0100081205011521fi (1 2008-1205-0852-0088-5279HI, f: 2008-12-05Z fj: 24kGB/T 476-2008GB/T 476-2008#,FTM4T7ftHTlT1 19F a7:Jr i 16ifs C =ire Pj: 10004 5nf1F www. spc. net. cn1L i,Ti :68523946 68517548f fif, d JftA“,EpFP9Il011FPI1A4 880X1230 1/16 Ep j5 1.25 f= C 28 fY2008 11) V -J,fi 2008 4r. 11 )1 s,-(J EphlJ15-0i: 155066 1-34269PQ 4T EP ;I V9 Fh *fifaTirp,biJ1#gv-v %V* 9,5;,#f fit:( 010)68533533
