1、 1FHZHJSZ0041 a F-HZ-HJ-SZ-0041 a 1 a B a P 0.004g/L B a P B a P 2 B a P 3 3.1 B a P 5.0mg B a P 50mL B aP 100g/mL 10g/mL 3.2 15 30cm 15 20 15cm 1000mL+=750mL+250 mL+0.5mL 55 1 6h 34 23 4h 3.3 367nm 10nm 2nm 405nm 3.4 3.5 3.6 3.7 3.8 3.9=1.84g/mL 3.10 3.11 DMSO 500mL 50mL 4 4.1 10mm 4.2 365nm 254nm
2、4.3 4.4 4.5 4000r/min 4.6 1L 3L 100mL 4.7 250mL 24.8 4.9 4.10 5mL 4.11 4.12 0.01mg 5 24h 6 6.1 6.1.1 2000mL 3000mL 50mL 3min 6.1.2 1000mL 1000mL 50mL 3min 6.1.3 2050g 12h 100mL 7075 KD 3 0.05mL 6.1.4 30cm 3cm 1.5cm 2.4 cm B a P 34 mm 4 4 1 1cm 24h B a P Rf 5mL 105110 10min 1min 300r/min 2min 6.2 B a
3、 P 10mm 10nm 2nm 367nm 402nm 405nm 408 nm F 7 B a P B a P B a P C 2408 402405nm nmnmF FF F+-=3 C B a P g/L M B a P g F B a P F V L R 8 8.1 B a P 0.2g L 1 1 1 0.230 6.9 2 0.199 8.0 3 0.213 13.0 4 0.202.6.6 5 0.179 4.2 8.2 2 3 2 1 107.0 6.9 2 93.3 8.0 3 121.0 13.0 4 99.0 6.6 5 73.3 4.2 3 1 79.8 4.4 2 83.0 12 3 81.4 7.6 4 93.3 6.2 9 GB 11895-1989 A1 6.1.2 100mL 20mL 100mL DMSO 2 5mL 2min DMSO 100mL 10mL DMSO RV FF MC=4 1 1HCl 15mL 2 5 mL 2min 10mL 100mL 5mL15 NaOH NaOH 23 15mL pH=7 KD 7 A2 B a P A3 A4 4h
