1、 14 4 2 0 0 8 M 1 2 s k / N ANALYSIS AND TESTING T ECH NOLOGY AND INSTRU M ENT SVolume 14 Number 4null null null null Dec. 2008 (241 247) ; s / y s 刘发龙,马新刚,程福银,何峻荣(中国航天科技集团公司四院四十二所,湖北襄樊null 441003)K null 1 : e 1 ; a+ ,8 ; j ? C ( 1978 null ) , 3 , = , V 3 , 1 V Y % 8 w 4 s k / .s k / N 14 1 s “ d ,
2、“ d ; E s s a c , ,Z E a y , V y s ) . YandeLiu 8 Q ; E H T $ aT # c , T a V L ,Z E y ad + , v v y H PLCE . Luypaert J 9 ; K l = E y s 4 e aaV 8 c N s . M ouazen A M 10 ! 9 B r L s “ d , Q ; y s r pH a a# s c N r ? . ? V 11 Q ; E H s aY Y c , Z E a y . E . 12 ; s / 9 a9 ac ,Z E y a ,X C s .1. 2null
3、J 5 ; J 5 y s 9 d a apH a = , Z E V y . Fei Liu 24 | V n / ; Z L s ,Z E a y , d + .1. 3null 0 5 ; 0 ? C , : ; s / y s r F s y Z E , L , Z E ? 9 0 y a s , 0 ? C , : ; s / y s 14 null H aiyan Cen, Yong H e. M easurement of soluble solidscontents and pH in orange juice using chemometricsand VisnullNIRS
4、 J . J Agric Food Chem, 2006, 54( 20) : 7 437null7 443. 15 null M aria G M acedo, M arienull france Laporte. Quantificnullation of exopolysaccharide, lact ic acid, and lactoseconcentrations in culture broth by nearnullInfraredspectroscopy J . J Agric Food Chem, 2002, 50( 7) : 1774null1 779. 16 null
5、Armenta S, Garrigues S. Determination of edible oilparameters by near infrared spectrometry J .Analytica Chimica Acta, 2007, 596: 330null337. 17 null , . 1 s ; E J . s , 2004, 32( 8) : 1 070null1 073. 18 null Sandra E Kays. Nearnull inf rared analysis of soluble andinsoluble dietary fiber fractions
6、of cereal foodproducts J . J Agric Food Chem, 2002, 50: 3 024null3029. 19 null u , f c r . ; _ C . = N / # “ ,2007. 47null49. 20 null Yiqun H uang, Todd M Rogers. Det ection of sodiumchloride in cured salmon roe by SWnullNIR spectroscopy J . J Agric Food Chem, 2001, 49: 4 161null4 167. 21 null Laura
7、 Alessandrini. Near inf rared spectroscopy: Ananalytical t ool to predict coffee roast ing degree J .Analytical chimica act a, 2008, 625: 95null102. 22 null H ect or R Juliani. Application of nearnullinfraredspectroscopy in qualit y control and determination ofadulteration of African essential oils
8、J . PhytochemAnal, 2006, 17: 121null128. 23 null Savenije B. Predict ion of pork quality using visible/nearnullinfrared ref lectance spectroscopy J . M eatScience, 2006, 73: 181null184. 24 null Fei Liu. Classification of brands of instant noodlesusing Vis/ NIR spectroscopy and chemomet rics J .Food
9、Research International, 2008, 41: 562null567. 25 null M erckle P, Kovar K A. Assay of effervescent tabletsby NearnullInfrared Spectroscopy in t ransmittance andreflectance mode: acetylsalicylic acid in mono andcombinat ion formulations J . J Pharm Biomed Anal,1998, 17: 365null374. 26 null Andersson
10、M , Josefson M . M onitoring of a filmcoating process for tablets using near infraredspectroscopy J . J Pharm Biomed Anal, 1999, 20: 20null30. 27 null U lmschneider M , Penigault E. Direct identification ofkey intermediates in containers using Fouriernulltransform nearnullinfrared spectroscopy throu
11、gh theprotect ive polyethylene primary packaging J .Analusis, 2000, 28( 2) : 136null140. 28 null Xiangji Zhou, Patricia H ines. M oisture determinationin hygroscopic drug substance by near infraredspectroscopy J . J Pharm Biomed Anal, 1998, 17:219null225. 29 null Berntsson O, Zackrisson G. Determina
12、t ion ofmoisture in hard gelatin capsules using nearnullinfraredspectroscopy: application to atnullline process control ofpharmaceutics J . J Pharm Biomed Anal, 1997, 15:895null900. 30 null John P Higgins, St even M Arrivo. Spectroscopicapproach of onnullline monit oring of particle size duringthe p
13、rocessing of pharmaceutical nanopart icles J .Anal Chem, 2003, 75( 8) : 1 777null1 785. 31 null Sonja Sekulic S, H oward W W ard. Onnulllinemonit oring of pow der blend homogeneity by nearnullinfrared spectroscopy J . Anal Chem, 1996, 68: 509null513. 32 null Li W Y. Determination of polymorph conver
14、sion ofan act ive pharmaceut ical ingredient in w et granulationusing NIR calibration models generated from thepremix blends J . J Pharm Sci, 2005, 94( 12) : 2 800null2 806. 33 null Z , . Q ; E x 3 ac J . s e , 2004, 32( 4) :477null480. 34 null , + . ; E y s J .C N , 2001, 5: 21null23. 35 null 2 , Z
15、 . ; y 9 0 Z E J . v ( ) , 2002, 36( 4) :463null466. 36 null Narve Aske, H arald Kallevik. Determination ofsaturate, aromat ic, resin, and asphaltenic ( SARA)component s in crude oils by means of infrared andnear- infrared spectroscopy J . Energy y J . s e , 2001, 29( 1) : 87null91. 38 null b . L ;
16、E _ Q Y Q( s / y s Application of NearnullInfraredSpectroscopy AnalyticalTechnique in Rapid AnalysisLIU Fanulllong, M A Xinnullgang, CH ENG Funullyin, H E Junnullrong( The 42nd Institute of the Four th Academy of CASC, Xiangfan 441003, China)Abstract: The principle and the char acteristics of near i
17、nfr ared spectr oscopy( NIRS) are presented briefly inthis paper. The research and application actualities of NIRS rapid analysis in agr iculture, food,pharmaceutical, petr ochemical industry, polymer and so on is summarized. T he application pr ospect ofNIRS is also proposed.Keywords: nearnullinfra
18、red spectr oscopy; rapid analysisClassifying number: O657. 32h 2009 M s k / N !null T X s k 5 Z _ s k T7 ? s k T / Z E Z s k N o ? s k N F q. . . . . . . . .h _ S = 7 ? s k / N ! , | ISSN 1006- 3757CN 62- 1123/ O6, ? | : 54- 90, N 8 / , M N 32 . g h s k / N !I “ , “ : ( 0931) 4968280, Enullmail: fxcs lzb. ac. cn, “ :f k , : 8 g ? 18| , S S .247
